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Título: Extracción Acelerada con Solventes de Residuos de Pesticidas en Productos Alimenticios.

Título original: Accelerated Solvent Extraction of Pesticide Residues in Food Products

Autor: Thermo Scientific.

Tipo de recurso: Nota de Aplicación

Introduction:

Residue analysis in crops and food products is routinely performed in regulatory and industrial laboratories around the world. Many of the traditional procedures used to perform these extractions are time-consuming and solvent-intensive. Accelerated solvent extraction is an extraction technique that speeds the extraction process and reduces the total amount of solvent used. The system uses conventional liquid solvents at elevated temperatures and pressures, which results in increased extraction kinetics. Extraction of samples ranging from 1 to 30 g typically requires 12–17 min and 15–50 mL of solvent. In the environmental industry, accelerated solvent extraction has been compared extensively to traditional preparation techniques, and has been found to generate similar extracts in a more efficient manner. Accelerated solvent extraction is now widely used in environmental applications to replace time- and solvent-intensive techniques such as Soxhlet and sonication. The principles of accelerated solvent extraction technology are based on conventional liquid extraction theory, so the transfer of existing solvent-based extraction processes to accelerated solvent extraction is simple. In addition, the ability to extract up to 24 samples unattended can result in a dramatic increase in laboratory efficiency.

 

Sample Preparation

Weigh dry samples (1–20 g) and add directly to extraction cells containing a cellulose extraction filter. Grind wet samples (1–10 g) and mix with 6 g of Dionex ASE™ Prep DE (diatomaceous earth) using a mortar and pestle. Rinse the mortar and pestle with 2–3 mL of the extraction solvent. Add this volume to the sample in the extraction cell.

 

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